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Sodium Bifluoride Oxygen difluoride was first reported in 1929; it was obtained by the electrolysis of molten potassium fluoride and hydrofluoric acid containing small quantities of water.[2][3] The modern preparation entails the reaction of fluorine with a dilute aqueous solution of sodium hydroxide 2F2 + 2NaOH - OF2 + 2NaF + H2O
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