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Iodobenzene Diacetate The first hypervalent iodine compound, dichloroiodobenzene (C6H5Cl2I) was prepared in 1886 by the German chemist C. Willgerodt [1] by passing chlorine gas through iodobenzene in a cooled solution of chloroform. C6H5I + ICl3 , C6H5ICl2 + ICl
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